High hydrostatic pressure equipment for neutron scattering studies of samples in solutions

• Verfasst von: Peters, Judith [VerfasserIn]
• Verfasst von: Trapp, Marcus [VerfasserIn]
• Titel: High hydrostatic pressure equipment for neutron scattering studies of samples in solutions
• Verf.angabe: Judith Peters, Marcus Trapp, Darren Hughes, Steven Rowe, Bruno Demé, Jean-Luc Laborier, Claude Payre, Jean-Paul Gonzales, Simon Baudoin, Nadir Belkhier, Eddy Lelièvre-Berna
• Jahr des Originals: 2011
• Umfang: 6 S.
• Fussnoten: Published online: 08 Dec 2011 ; Gesehen am 30.07.2018
• Titel Quelle: Enthalten in: High pressure research
• Jahr Quelle: 2012
• Band/Heft Quelle: 32(2012), 1, S. 97-102
• ISSN Quelle: 1477-2299
• DOI: doi:10.1080/08957959.2011.642376
• Datenträger: Online-Ressource
• Sprache: eng
• K10plus-PPN: 1578073995

Abstract

The design of new high pressure equipment for structural and dynamical studies on samples in solution is described. We present two sample cells for applying pressures up to 150 and 700 MPa (i.e. 1.5 and 7 kbar), respectively. These cells are mounted on special sticks and inserted into the calorimeter of a cryostat to regulate the temperature. Different parts of the equipment - the pressure controller, the sticks and the cells - are described. In addition, radiography tests which were performed with neutrons in situ at the Institut Laue Langevin to verify the tightness of the cells and the hydrostatic transmission of the pressure to the sample are presented. First results on model lipids are in agreement with former results by R. Winter et al. [Towards an understanding of the temperature/pressure configurational and free-energy landscape of biomolecules, J. Non-Equilib. Thermodyn. 32 (2007), pp. 41-97].